Chemistry Lab Protocols / Classical techniques
Performing a titration
Add one or two drops of indicator to the titrand contained in the conical
flask. For a right-handed person the process is as follows:
- Hold the conical flask containing the tit rand and the indicator in your
right hand, and control the tap of the burette with your left hand. The
burette should be arranged so that the tap is on the opposite side of the
burette to your palm. In this way, your left hand also supports the body
of the burette.
- Add the titrant by opening the tap, and simultaneously swirl the contents
of the conical flask. This may take a bit of practice, so do not worry if
you cannot do it straight away. The titrant can be added quickly at first,
but as the end-point approaches, additions should be made drop-wise.
- The end-point is indicated when the appropriate colour change takes
place. When the end-point is reached, one drop of titrant should be
sufficient to cause the colour change. You should note the volume used
for the titration to the nearest 0.1-D.05mL. This is done by reading off
the volume of titrant used.
- Refill the burette to the zero mark using a funnel ready for the next
titration.
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