Chemistry Lab Protocols / Fundamental laboratory techniques
Safety with glass
Many minor accidents in the laboratory are due to lack of care with
glassware. You should follow these general precautions:
- Wear eye protection at all times.
- Don't use chipped or cracked glassware and examine the equipment for
'star' cracks - it may break under very slight strains and should be disposed
of in the broken glassware bin. All laboratories will have a waste bin
dedicated to broken glass. Never put broken glass into other bins.
- If heating glassware, use a 'soft' Bunsen flame (half-open air vent) or
'wave' the flame around the heating point - this avoids creating a hot
spot where cracks may start. Always use special heat-resistant gloves or
rubber 'fingers' when handling hot glassware.
- When clamping glassware ensure that the clamp has a cork,
rubber or plastic 'cushion' in the jaws to prevent breakages. There must
be no metal-glass contact and you must not over-tighten the clamp.
- Take care when attaching rubber or plastic tubing to glass tubes,
condensers, etc., and inserting thermometers and glass tubes into
screwcap adapters. Always hold the tube and the 'hole' close
together (Fig. 3.5) and wear thick gloves where appropriate.
- Don't force bungs too firmly into bottles they can be difficult
to remove. If you need a tight seal, use a screwtop bottle, with a rubber
or plastic seal, Parafilm® or ground-glass jointware, such as Quickfit®.
- Never carry large bottles (> 1L) by their necks - carry them in a bottle
basket.
- Dispose of broken glass thoroughly and with great care - use disposable
paper towels, tongs or dust-pan and brush and thick gloves. Always put
pieces of broken glass in the correct bin.
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